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The structure of 2,2'-diphenyl-1,1'-(1,4-phenylene)diethanedione, C22H14O4

✍ Scribed by Syed, A. ;Stevens, E. D.


Book ID
114502315
Publisher
International Union of Crystallography
Year
1984
Tongue
English
Weight
444 KB
Volume
40
Category
Article
ISSN
0108-2701

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Synthesis of phenyl [1-14C]acetylene and
✍ Som N. Dhawan; Jacques Kagan πŸ“‚ Article πŸ“… 1982 πŸ› John Wiley and Sons 🌐 French βš– 218 KB

## Abstract Phenyl [1‐^14^C] acetylene (0.012mCi/mmole) was synthesized in 12.5% yield from [1‐^14^C] acetic acid through [1‐^14^C] acetophenone, its semicarbazone, and 4‐phenyl‐[4‐^14^C] 1,2,3‐selenadiazole obtained by selenium dioxide oxidation. Oxidative coupling gave 1,4‐diphenyl [1,4‐^14^C~2~]