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The Stevens rearrangement of isoquinolinium salts. A novel synthesis of 1-benzyl-1,2,3,4-tetrahydroisoquinolines.

✍ Scribed by Guenter Grethe; Hsi Lin Lee; Milan R. Uskoković

Publisher
Elsevier Science
Year
1969
Tongue
French
Weight
208 KB
Volume
10
Category
Article
ISSN
0040-4039

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The synthesis of Qastaeomerieally pure (-)\_(S) ~lhyl 2-metboxy-l-naphthalenesulfurab (5) is (+)-(R) benzyl zmethoxy+napbthy1 sulfoxidc. (7) and (8) rcspd't?y. in hi@ coimtiomeric ~&h&d (8) &erg-additkm IO 6,7-dSmetboxy-3.4diby N-oxide (2) to give a l-be=@-i23.~ tetranydroisoq~ ddvative (9) with big