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The small-scale synthesis of 13-labelled dichloromethylphosphine (methylphosphonous dichloride)

✍ Scribed by I. J. Colquhoun; W. McFarlane

Publisher: John Wiley and Sons
Year: 1977
Tongue: French
Weight: 111 KB
Volume: 13
Category: Article
ISSN: 0022-2135
DOI: 10.1002/jlcr.2580130410

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✦ Synopsis

THE SMALL-SCALE SYNTHESIS OF 13C-18ARELLED DICHLOROMETHV, PHOSPHIXE (METHYLPHOPPHONOUS DICHLORIDE) I a J.Colqutboun and :I .Plck'arlane, Department of Chemistry, C i t y o f London Polytechnic, London 5X3N 2EY, tingland.

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✍ Dr. J. D. Kennedy 📂 Article 📅 1975 🏛 John Wiley and Sons 🌐 French ⚖ 92 KB

In connection'with other studies, we have synthesised methyltin triiodide and trimethyltin iodide enriched with I3C in the methyl groups. methods of equations ( 1)-( 4) and ( 5) were adequate, and the most satisfactory procedures were as described below. The SnC12