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The simple preparation of mevalonic-3′, 4-D Acid and -3′, 4-T Acid

✍ Scribed by Mitsuyoshi Matsuo; Yosihiko Kasida


Book ID
102373903
Publisher
John Wiley and Sons
Year
1968
Tongue
French
Weight
190 KB
Volume
4
Category
Article
ISSN
0022-2135

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✦ Synopsis


Mevalonic-3', 4 -0 acid and -3', 4-T acid were synthesized by using deuterated and tritiated water und the total yield of the labelled M V A was 6.5 %. The specijc activity of the tritiated M V A , which was derived ,from 2.3 g. of tritiated water (250 mCi), MYZS 1.77 mCi.linM.


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Single-crystal X-ray study T = 290 K Mean (C-C) = 0.005 A R factor = 0.069 wR factor = 0.159 Data-to-parameter ratio = 12.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.