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The reactions of ω-(phenylthio)acetophenone

✍ Scribed by Teruaki Mukaiyama; Toshiyuki Takashima; Syohachi Ono

Publisher
Elsevier Science
Year
1967
Tongue
French
Weight
172 KB
Volume
8
Category
Article
ISSN
0040-4039

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Titanocene(II)-Promoted Olefination of ω
Titanocene(II)-Promoted Olefination of ω,ω-Bis(phenylthio)alkyl Alkanoates. A New Method for the Preparation of ω-Hydroxy Ketones
✍ Md.Abdur Rahim; Tooru Fujiwara; Takeshi Takeda 📂 Article 📅 2000 🏛 Elsevier Science 🌐 French ⚖ 215 KB

Intramolecular olefination of esters having a thioacetal moiety was studied. The treatment of v,v-bis(phenylthio)alkyl alkanoates with Cp 2 Ti[P(OEt) 3 ] 2 and the following hydrolysis gave v-hydroxy ketones in good yields.