The reaction of ethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate with fullerene C60
✍ Scribed by N. F. Gol'dshleger; A. S. Astakhova; A. S. Lobach; G. N. Boiko; N. N. Denisov; V. A. Nadtochenko; O. S. Roshchupkina; Yu. M. Shul'ga
- Book ID
- 112537850
- Publisher
- Springer
- Year
- 1996
- Tongue
- English
- Weight
- 357 KB
- Volume
- 45
- Category
- Article
- ISSN
- 1573-9171
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📜 SIMILAR VOLUMES
In the optically active title compound, C 32 H 30 N 2 O 8 , the substituted 1,4-dihydropyridine ring adopts a flattened boat conformation. The crystal structure is stabilized by intermolecular N-HÁ Á ÁO hydrogen bonding. ## Data collection Bruker SMART 1000 CCD diffractometer Absorption correctio
In the molecule of the title compound, C 21 H 28 N 2 O 5 , the substituted 1,4-dihydropyridine (1,4-DHP) ring has a flattened-boat conformation. The carbonyl groups of the ester groups, at positions 3 and 5 in the 1,4-DHP ring, have cis configurations with respect to the double bonds in the 1,4-DHP
Single-crystal X-ray study T = 113 K Mean (C-C) = 0.002 A Disorder in solvent or counterion R factor = 0.044 wR factor = 0.120 Data-to-parameter ratio = 14.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.