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(R*)-(−)-3-[4-(Benzyloxy)benzoylmethyl] 5-ethyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate

✍ Scribed by Wu, Xiao-Yun ;Hu, Ai-Xi ;Cao, Gao

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
587 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis

In the optically active title compound, C 32 H 30 N 2 O 8 , the substituted 1,4-dihydropyridine ring adopts a flattened boat conformation. The crystal structure is stabilized by intermolecular N-HÁ Á ÁO hydrogen bonding.

Data collection

Bruker SMART 1000 CCD diffractometer Absorption correction: none 5566 measured reflections 2808 independent reflections 1747 reflections with I > 2(I)

1.02 2808 reflections 382 parameters 3 restraints H-atom parameters constrained Á max = 0.21 e A ˚À3 Á min = À0.21 e A ˚À3

Table 1

Hydrogen-bond geometry (A ˚, ).

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