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The Reaction of 2-Chlorocyclohexanone with β-Naphthol. A Novel Synthesis of γ-Brazan

✍ Scribed by Osdene, T. S.; Russell, Peter B.

Book ID
127203407
Publisher
American Chemical Society
Year
1966
Tongue
English
Weight
440 KB
Volume
31
Category
Article
ISSN
0022-3263

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## a b s t r a c t The sulfoxide-magnesium exchange reaction of aryl 1-chlorocyclopropyl sulfoxides with i-PrMgCl in THF at low temperature gave magnesium cyclopropylidenes. Treatment of the magnesium cyclopropylidenes with lithium naphtholates or phenolates resulted in the formation of spiro[2.6]n