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The Protonation of HSO3F: Preparation and Characterization of Fluorodihydroxyoxosulfonium Hexafluoroantimonate [H2SO3F]+[SbF6]−

✍ Scribed by Raphael Seelbinder; Nadine R. Goetz; Johannes Weber; Rolf Minkwitz; Andreas J. Kornath

Publisher
John Wiley and Sons
Year
2009
Tongue
English
Weight
281 KB
Volume
16
Category
Article
ISSN
0947-6539

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The Protonation of CF3SO3H: Preparation
The Protonation of CF3SO3H: Preparation and Characterization of Trifluoromethyldihydroxyoxosulfonium Hexafluoridoantimonate, CF3SO3H2+SbF6–
✍ Theresa Soltner; Nadine R. Goetz; Andreas Kornath 📂 Article 📅 2011 🏛 John Wiley and Sons 🌐 English ⚖ 460 KB

Trifluoromethanesulfonic anhydride reacts with superacidic solutions AF/SbF 5 (A = H, D) to form their corresponding salts CF 3 SO 3 A 2 + SbF 6 -, which are protonated forms of trifluoromethanesulfonic acid and CF 3 SO 2 F as by-product. The salts have been characterized by vibrational spectroscopy