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The Preparation of N-(Dialkylaminoalkyl) Diacetamides†

✍ Scribed by Klayman, Daniel L. ;Smith, Pierre F.


Book ID
102410455
Publisher
Elsevier
Year
1953
Weight
172 KB
Volume
42
Category
Article
ISSN
0095-9553

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The Preparation of α-(Dialkylaminoalkyl)
✍ Nightingale, Dorothy; Ungnade, H. E.; French, H. E. 📂 Article 📅 1945 🏛 American Chemical Society 🌐 English ⚖ 383 KB

A portion of the above picrate was treated with an excess of 6 N HCl, and the precipitated picric acid was filtered off. The acid filtrate was extracted with ether to remove traces of picric acid. The aqueous layer was chilled in ice, and enough sodium hydroxide wa5 added to rnakc the mixture just a