The Preparation of [15N,15N']-and [4,4'-13 C2]-4,4'-Dichloroazobenzene and [ , Nt]-4-Chloroazobenzene 15N 15
THE PREPARATION OF N 15 -BUTYLACETAMIDE AND ITS N 15 -D DERIVATIVE
✍ Scribed by VAUGHAN, W. R.; ANDERSEN, M. V.; BLANCHARD, H. S.; McCANE, D. I.; MEYER, W. L.
- Book ID
- 120442475
- Publisher
- American Chemical Society
- Year
- 1955
- Tongue
- English
- Weight
- 323 KB
- Volume
- 20
- Category
- Article
- ISSN
- 0022-3263
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## Abstract Phenoxybenzamine [N‐Bethyl‐N‐(l‐phenoxyisopropyl)‐2‐chloroethylamine hydrochloride] has been labelled with Nitrogen‐15 by a direct synthesis from ^15^N‐ammonium chloride. The isotopic enrichment was 92.8%.
## Abstract The production of L‐glutamic acid‐^15^N in good yield by direct enzymic synthesis from 2‐oxoglutaric acid, ammonium chloride‐^15^N (95 atom % ^15^N) and reduced nicotinamide adenine dinucleotide phosphate (NADPH) is described. The NADPH is continuously regenerated by coupling the first