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The Preparation of Methoxysilanes by the Interaction of Monosilane and Methanol 1

✍ Scribed by Sternbach, Burt; MacDiarmid, Alan G.

Book ID: 121188620
Publisher: American Chemical Society
Year: 1959
Tongue: English
Weight: 211 KB
Volume: 81
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja01528a023

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A portion of the above picrate was treated with an excess of 6 N HCl, and the precipitated picric acid was filtered off. The acid filtrate was extracted with ether to remove traces of picric acid. The aqueous layer was chilled in ice, and enough sodium hydroxide wa5 added to rnakc the mixture just a