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The Preparation of Fluorocarbon Carboxylic Acid “Thiocyanates” 1

✍ Scribed by Patton, R. H.; Simons, J. H.

Book ID
121265158
Publisher
American Chemical Society
Year
1955
Tongue
English
Weight
143 KB
Volume
77
Category
Article
ISSN
0002-7863

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Pictet-Spengler condensation of dopamine with (+)-menthyl pyruvate afforded a diastereomeric mixture of menthyl salsolinol-l-carboxylate, from which pure diastereomer was isolated by repeated recrystallizations in ca. 20% yield. Acid hydrolysis of the menthyl ester furnished (-)-(R)-salsolinol-l-car