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THE PREPARATION OF A FORMALDEHYDE ADDUCT OF 3-DIMETHYLAMINO-2,2-DIMETHYLPROPIONALDEHYDE

✍ Scribed by Taylor, Lloyd D.; McLaughlin, Paul; Mach, Martin

Book ID
120234723
Publisher
Informa UK (Taylor & Francis)
Year
1970
Tongue
English
Weight
138 KB
Volume
2
Category
Article
ISSN
0885-6672

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The Reaction of 3-(Dimethylamino)-2H-azi
The Reaction of 3-(Dimethylamino)-2H-azirines with 2,3-Pyridinedicarboximide
✍ Jean-Pierre Obrech; Peter Schönholzer; Christain Johannes Jenny; Roland Prewo; H 📂 Article 📅 1988 🏛 John Wiley and Sons 🌐 German ⚖ 512 KB

Reaction of 2,2-dialkyl-3-(dimethylamino)-2H-azirines la and l b with 2.3-pyridinedicarboximide (4) in MeCN or DMF at room temperature yielded two regioisomeric tricyclic 1:l adducts, the azacyclols 11/12 and 16/17, respectively (Schemes 3 and 4 ) . The structure of 12 was established by X-ray cryst