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The preparation of 2: 6-Dimethylheptadiene

✍ Scribed by H. I. Waterman; W. J. C. de Kok

Publisher
Elsevier Science
Year
2010
Tongue
English
Weight
266 KB
Volume
52
Category
Article
ISSN
0165-0513

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A simple and efficient preparation of 2,
A simple and efficient preparation of 2, 2, 6, 6- tetradeuteriocyclohexanone
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## R e c e i v e d on M a y 2 3 , 1973 1 The preparation of 2,2,6,6-tetradeuteriocyclohexanone is reported using a 10 % DCI-D PO exchange solution, generated from PC15 and D20. Another p r ~c e d u r e ~~u s : ~ a K CO -0 0 exchange solution,which results in a significant amount of base-catalyzed

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## Abstract The preparation of 2 :4 : 6‐trinitrobenzoic acid by the oxidation of 2:4:6‐trinitrotoluene (TNT) in nitric acid solution with sodium chlorate, by the method of LΓΌttgen,^1^ has been rightly condemned by Clarke and Hartman^2^ on the grounds of control difficulty. However, it has been foun