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The preparation and Raman spectroscopic study of the chlorotetrafluorosilicate (IV) ion, SiF4Cl−

✍ Scribed by H.G.M. Edwards; V. Fawcett; S.J. Rose; D.N. Smith

Publisher
Elsevier Science
Year
1992
Tongue
English
Weight
652 KB
Volume
268
Category
Article
ISSN
0022-2860

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## Abstract Raman spectra of oriented single crystals of (NH~4~)~2~SiF~6~ are reported for the temperature range 440–20 K. The trigonal phase stable below 278 K undergoes a transition at 38.6 K. The changes in the spectra show that the symmetry does not remain trigonal, but give evidence for a lowe