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The Preparation and C-20 Configuration of the 5α,17α-Pregnane-3β,20-diols 1

✍ Scribed by Glick, David M.; Hirschmann, H.

Book ID
126136913
Publisher
American Chemical Society
Year
1962
Tongue
English
Weight
849 KB
Volume
27
Category
Article
ISSN
0022-3263

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Synthesis of 5α-pregnane-3β,20α-diol and
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✍ T. A. Baillie; J. E. Herz; J. Sjövall 📂 Article 📅 1974 🏛 John Wiley and Sons 🌐 French ⚖ 241 KB 👁 1 views

## Abstract A convenient synthesis of 5α‐[20β‐^2^H]pregnane‐3α,20α‐diol and 5α‐[20β‐^2^H]pregnane‐3β,20α‐diol from 3β‐hydroxy‐5α‐pregn‐16‐en‐20‐one is described. The reaction products are characterized by combined gas chromatography‐mass spectrometry.