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The Polymerization of Styrene by n-Butyllithium 1

✍ Scribed by Welch, F. J.

Book ID
127084598
Publisher
American Chemical Society
Year
1959
Tongue
English
Weight
466 KB
Volume
81
Category
Article
ISSN
0002-7863

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## Abstract The polymerization of styrene by __n__‐butyllithium and titanium tetrachloride has been examined. Isotactic polystyrene is obtained only when 3.00 > __n__‐BuLi/TiCl~4~ > 1.75. At ratios less than 1.75 and greater than 3.00 only amorphous polystyrene (soluble in MEK) was formed. The mole

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The polymerization of styrene catalyzed by n-butyllithium has been carried out in the presence of carbon black at 0°C in toluene. A large portion of the catalyst was consumed by the reaction with the carbon black surface and thus the growth of polystyrene anions on the surface was hindered to a cons