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The nature of the anchimeric assistance by the acetoxy group in solvolysis of (Me3Si)2C(SiMe2)OCOMe) (SiMe2Cl)

✍ Scribed by Colin Eaborn; Paul D. Lickiss; Alan D. Taylor

Publisher: Elsevier Science
Year: 1988
Tongue: English
Weight: 225 KB
Volume: 338
Category: Article
ISSN: 0022-328X
DOI: 10.1016/0022-328x(88)80516-3

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## Abstract The reaction of __N,N′,N′′__‐trimethyl‐1,3,5‐triazacyclohexane chromium trichloride ((Me~3~TAC)CrCl~3~, 1) with LiN(SiMe~3~)~2~ or NaN(SiMe~3~)~2~ in petroleum ether yields nearly quantitatively [Cr{N(SiMe~3~)~2~}~3~] (2) with loss of the Me~3~TAC ligand. Compound 2 could be crystallize