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The First α-Fluoroallenylphosphonate, the Synthesis of Conjugated Fluoroenynes, and the Stereoselective Synthesis of Vinylfluorophosphonates Using a New Multifunctional Fluorine-Containing Building Block

✍ Scribed by Zapata, Antonio J.; Gu, Yonghong; Hammond, Gerald B.

Book ID
120190564
Publisher
American Chemical Society
Year
2000
Tongue
English
Weight
357 KB
Volume
65
Category
Article
ISSN
0022-3263

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37 8C) and the mixture was filtered in a UltraFree MC 30 000 MWCO centrifugal filtration unit (Millipore) at 3500 g for 7 min at 37 8C. The concentration of free substrate in the filtrate was quantified by ICP-MS and the bound fraction was calculated as % bound ([total]-[free])/[total]. The proton T