✦ LIBER ✦

The First Clamped and Strongly Deformed Adamantane

✍ Scribed by Prof. Dr. Fritz Vögtle; Dipl.-Chem. Joachim Dohm; Dr. Kari Rissanen

Publisher: John Wiley and Sons
Year: 1990
Tongue: English
Weight: 380 KB
Volume: 29
Category: Article
ISSN: 0044-8249
DOI: 10.1002/anie.199009021

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✦ Synopsis

l-Butyl-2,3,4-tri-terr-butyl-l,3,2,4-diazadiboretidine, 4. Compound 1 (0.80 g) and butyl azide (0.39 g) were combined in 10 mL of pentane at 0 "C and the resulting solution was stirred for 30 min at room temperature. Distillative workup gave 4 (0.70 g, 65%) as a colorless liquid at 70 'C/O.Ol Torr.

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