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The electron spin resonance spectrum of the triphenylsilyl radical formed by the X-irradiation of monocrystalline triphenylsilane

✍ Scribed by M. Geoffroy; E. A. C. Lucken

Publisher
John Wiley and Sons
Year
1970
Tongue
German
Weight
327 KB
Volume
53
Category
Article
ISSN
0018-019X

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✦ Synopsis

Normaldruck hydriert. Man filtrierte und dampfte ab. Nach Zusatz von alkoholischer Salzsaure und erneutem Abdampfen erhielt man aus Isopropanol-Ae 1,l g (92%) farblose Prismen, Smp. 159-160", die nach Misch-Smp., 1R.-und NMR.-Spektrum identisch waren mit 2-Methyl-3-dimethylamino-

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