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The effect of particle size distributions on the CRSS of aged NiAl alloys

✍ Scribed by V. Munjal; A.J. Ardell


Publisher
Elsevier Science
Year
1976
Weight
738 KB
Volume
24
Category
Article
ISSN
0001-6160

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✦ Synopsis


The effect of the width of the 7' particle size distribution on the CRSS of Ni-AI single crystals containing nominally 6 wt.>; Al was investigated. The samples were given two-step aging treatments to produce broader unimodal distributions than those resulting from isothermal aging. The first aging treatments were done at 600 and 650°C for 458 and 69 hr, respectively, while the second were done at 625'C for various lengths of time. In all the samples the average particle size was nearly constant. but the standard deviation, b. was increased by as much as 300/,, primarily by the addition of smaller precipitates. After correcting for variations in the 7' volume fraction introduced by these treatments, the effect of increasing D was to reduce the CRSS of the samples by approx. So& This change, which is very small, is nevertheless substantially larger than that predicted by the computer experiments of Foreman and Makin. It is suggested that the discrepancies are due to the shortcomings of modelling real precipitate dispersions by arrays of point particles.

R&urn&--On a ttudie I'effet de la largeur de repartition des tailles des particules 7' sur la CCR de monocristaux de Ni-AI contenant 6% d'aluminium en poids. On faisait subir aux echantillons un vieillissement en deux etapes afin de produire une repartition unimode plus large que celle que I'obtient par recuit isotherme. Les premiers recuits itaient de 488 et 69 h a 600 et 650°C respectivement, alors que les suivants Ctaient effectues a 625°C pendant des durees variables. La taille moyenne des particules etait a peu prts constante dans tous les ichantillons. mais la deviation standard u pouvait augmenter de 30?/,. essentiellement par I'addition de petits precipites. Apres correction pour la variation de la fraction volumique de ; ' introduite par ces traitements, on voit que l'augmentation de a produit une diminution de la CCR d'environ 8%. Ce changement est tres petit, il est toutefois nettement plus grand que celui prevu sur ordinateur par Foreman et Makin. Nous pensons que les differences proviennent de l'insuffisance de modele qui represente une repartition de pricipitts reels par un reseau de particules ponctuelles.

Zusammenfassuttg--Der

EinAuD der Breite der GroDenverteilung von v'-Partikeln auf die kritische FlieBspannung wurde an Ni-AI Einkristallen mit 6 Gew.-% Al Nominalgehalt untersucht. Die Proben wurden in zwei Stufen gealtert, urn breitere Verteilungen als bei isothermer Alterung zu erhalten. Die erste Stufe fand statt bei 600 und 650°C fur 488 und 49 h. die zweite bei 62X iiber verschieden lange Zeiten. In ailen Proben war die mittlere PartikelgrijBe nahezu konstant, die Standardabweichung e aber war 30'1; gro&r. vorw.iegend wegen der vorhandenen kleineren Ausscheidungen. Es ergab sich nach einer Korrektur wegen Anderungen im Volumenbruchteil der y'-Phase, die durch die Behandlung erzeugt worden yar, da8 das vergrijBerte G die kritische FlieDspannung der Proben urn etwa 8% erniedrigte. Diese Anderung ist zwar sehr klein, jedoch betrachtlich griil3er als die von den Computerexperimenten von Foreman und Makin vorhergesagte. Es liegt nahe, daD diese Diskrepanz von der Unzulanglichkeit einer Beschreibung einer realen Verteiiung von Ausscheidungen mit punkfiirmigen Teilchen herriihrt.


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