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The cyclization reaction of 5-hexenoyl chloride with tri-n-butyltin hydride

✍ Scribed by E.J. Walsh Jr.; J.M. Messinger II; D.A. Grudoski; C.A. Allchin

Book ID
108381892
Publisher
Elsevier Science
Year
1980
Tongue
French
Weight
183 KB
Volume
21
Category
Article
ISSN
0040-4039

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πŸ“œ SIMILAR VOLUMES

The free-radical reaction of tri-n-butyl
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## Abstract Rate constants for the tri‐__n__‐butyltin radical (**Sn Β·**) induced decomposition of a number of peroxides have been measured in benzene at 10Β°C. The values range from ∼100 __M__^βˆ’1^ sec^βˆ’1^ for di‐__t__‐butyl peroxide to 2.6 Γ— 10^7^ __M__^βˆ’1^ sec^βˆ’1^ for di‐__t__‐butyl diperoxyisophth

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The kinetics and absolute rate constants for the free-radical chain reaction of tri-nbutyltin hydride with di-t-butyl disulfide have been measured in cyclohexane at 30". The rate controlling step for chain propagation involves the cleavage of the disulfide bond by an attacking tributyltin radical. T