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The crystal structures of barium inosine-5'-phosphate and disodium inosine-5'-phosphate

โœ Scribed by Nagashima, N. ;Iitaka, Y.


Book ID
117856405
Publisher
International Union of Crystallography
Year
1968
Weight
194 KB
Volume
24
Category
Article
ISSN
0567-7408

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Synthesis of 14C-labeled inosine 5โ€ฒ-phos
โœ Shinji Sakata; Shiro Ikegami ๐Ÿ“‚ Article ๐Ÿ“… 1978 ๐Ÿ› John Wiley and Sons ๐ŸŒ French โš– 172 KB

I4C-Labeled inosine 5'-phosphate was synthesized by direct phosphorylation of i n 0 s i n e -8 -~~C with phosphoryl chloride followed by hydrolysis of the resulting phosphorodichloridate. Isolation and recrystallization o f its disodium salt afforded pure material in 66.8% overall chemical yield.