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The crystal structure of (phenylazophenyl-C,N')mercury(II) chloride: a dimeric rans-metallation reagent

✍ Scribed by Mushtaq Ali; William R. McWhinnie; Thomas A. Hamor


Publisher
Elsevier Science
Year
1989
Tongue
English
Weight
221 KB
Volume
371
Category
Article
ISSN
0022-328X

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The reaction of PhN 3 (H)C 6 H 4 N 3 (H)Ph with Hg(NO 3 ) 2 in THF in the presence of triethylamine yields {Hg[PhN 3 C 6 H 4 N 3 (H)Ph](NO 3 )} as a yellow powder that can be recrystallized from THF/acetone. The crystals belong to the monoclinic system, space group P2 1 with the cell dimensions a Ο­