The crystal structure analysis of deuterated benzene and deuterated nitromethane by pulsed-neutron powder diffraction: a comparison with single crystal neutron diffraction analysis
β Scribed by W.I.F. David; R.M. Ibberson; G.A. Jeffrey; J.R. Ruble
- Publisher
- Elsevier Science
- Year
- 1992
- Tongue
- English
- Weight
- 271 KB
- Volume
- 180-181
- Category
- Article
- ISSN
- 0921-4526
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β¦ Synopsis
The results of time-of-flight neutron powder diffraction analyses at 4.2 K are compared with those from steady-state neutron single-crystal analyses at 15 K for deuterated benzene, C,D,, and deuteronitromethane, CD,NO,.
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Two new compounds, Rb 2 (HSO 4 )(H 2 PO 4 ) and Rb 4 (HSO 4 ) 3 (H 2 PO 4 ), were synthesized from aqueous solutions of RbHSO 4 /RbH 2 PO 4 . The compounds were characterized by Xray single crystal analysis and neutron powder di4raction. For Rb 2 (HSO 4 )(H 2 PO 4 ), room temperature and a low tempe
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