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The crystal and molecular structures of axial–equatorial and axial–axial bis(4,6-dimethyl-2-thioxo-1,3,2-dioxaphosphorinanyl) oxide

✍ Scribed by Wieczorek, M. W. ;Sheldrick, W. S. ;Karolak-Wojciechowska, J. ;Mikołajczyk, M. ;Witczak, M. ;Ziemnicka, B.

Book ID
114526387
Publisher
International Union of Crystallography
Year
1979
Weight
523 KB
Volume
35
Category
Article
ISSN
0567-7408

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The crystal structure of the title compound (3) was determined by the X-ray diffraction technique from diffractometer intensity measurements: C,H, O& monoclin{c space group P2, c, a = 12.644( 1) A, b = 6.102(1) A, c = 12.920(2) 1, B = 110.78(1)", 2193 reflections, and R = 0.043. The molecule of 3 ad