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The Crystal and Molecular Structure of Hydroxybenzylpindolol

✍ Scribed by Hans Peter Weber; Trevor J. Petcher

Publisher
John Wiley and Sons
Year
1977
Tongue
German
Weight
277 KB
Volume
60
Category
Article
ISSN
0018-019X

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✦ Synopsis

Kristalline und molekulare Struktur von Hydroxybenzylpindolol

Im Zusammenhang mit einer Studie über die Konformation von adrenergen β‐Blockern wurde die kristalline Struktur von Hydroxybenzylpindolol durch Röntgen‐analyse bestimmt. Die Kristalle sind triklin, Raumgruppe __P__1, a = 10,041(2), b = 11,386(2), c = 10,131(2) Å, α = 114,03(2), β = 107,82(3), γ = 99,32(3)°, mit zwei Molekeln pro Zelle. Die Struktur wurde nach dem «Multisolution»‐Prinzip gelöst und bis zu R=0,050 verfeinert. Die Molekeln sind im Kristall durch ein Netz von Wassertoffbrücken miteinander verbunden.

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