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The Crystal and Molecular Structure of [Co(tmen)3](C7H7SO3)3·2 H2O and [Co(tmen)3](CH3SO3)2·EtOH·1/2 H2O (tmen = 2,3-dimethylbutane-2,3-diamine)

✍ Scribed by Hans Brunner; Andreas Ludi; Andrea Raselli; Hans-Beat Bürgi


Publisher
John Wiley and Sons
Year
1996
Tongue
German
Weight
177 KB
Volume
79
Category
Article
ISSN
0018-019X

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Synthesis, Crystal Structure, and Therma
✍ Mathias S. Wickleder 📂 Article 📅 2001 🏛 John Wiley and Sons 🌐 German ⚖ 172 KB 👁 2 views

La(CH 3 SO 3 ) 3 ´2 H 2 O was prepared by the reaction of La 2 O 3 with CH 3 SO 3 H. According to the X-ray single crystal determination, the compound crystallizes with triclinic symmetry (P 1, Z = 2, a = 524.99( 8), b = 1015.3(2), c = 1298.0(2) pm, a = 98.62(2)°, b = 91.12(2)°, c = 104.61(2)°, R al