✦ LIBER ✦

The correlation between the stereochemistry of some indole and oxindole alkaloids and their behaviour on thin layer chromatograms

✍ Scribed by J.D. Phillipson; E.J. Shellard

Publisher: Elsevier Science
Year: 1966
Tongue: English
Weight: 745 KB
Volume: 24
Category: Article
ISSN: 1873-3778
DOI: 10.1016/s0021-9673(01)98104-x

No coin nor oath required. For personal study only.

✦ Synopsis

Adsorbents: Aluminium oxide G (Merck, 15 y0 calcium sulphate), 35 g/60 ml distilled water; Silica gel G (Merck), 30 g/60 ml distilled water.

Plate size: 20 x 20 cm. Layer thickness: 250 t_l.

Activation: Air dried for 15 min, heated at rag O for 60 min, stored in a desiccator over silica gel and reheated for 15 min at 105~ immediately prior to use.

Solvents : See below ; freshly distilled. Running distance: IO cm. Temperature : 22

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