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The coordination chemistry of 2,2′-oxydibenzoic acid, 2,2′-thiobenzoic acid, 3,3′-oxydipropionic acid and 3,3′-thiodipropionic acid with selected first row transition metal ions

✍ Scribed by Barrie S. James; William R. McWhinnie

Book ID
104847452
Publisher
Springer
Year
1981
Tongue
English
Weight
649 KB
Volume
6
Category
Article
ISSN
0340-4285

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The first asymmetric synthesis of (2S)-, and (2R)-amino-3,3-dimethoxypropanoic acid (a-formylglycine dimethylacetal) has been achieved in two steps and 91% overall yield. The key step involved the quenching of a chiral glycine titanium enolate with trimethyl orthoformate.