The Complexed Triphosphaallyl Radical, Cation, and Anion Family
✍ Scribed by Manfred Scheer; Christian Kuntz; Markus Stubenhofer; Michael Linseis; Rainer F. Winter; Marek Sierka
- Publisher
- John Wiley and Sons
- Year
- 2009
- Tongue
- English
- Weight
- 432 KB
- Volume
- 48
- Category
- Article
- ISSN
- 0044-8249
No coin nor oath required. For personal study only.
📜 SIMILAR VOLUMES
200 mL) was acidified with 3 drops of 32% HCI and stirred for 15 min at 50°C (exclusion of light). After extraction with CH,CI,, the organic phase was dried (Na,SO,) and purified on silica gel (20 8). After removal of the solvent there remained 0.53 g (72%) of a crystalline product. For further puri
The radical cations and the radical anions of 1,6-dithiapyrene (1) and 3,lO-dithiaperylene (2) as well as those of three further Weitz-type S-donors 3,4, and 5 have been studied by ESR spectroscopy. The experimental findings for 1: (widths and behaviour on saturation of hyperfine lines) suggest that