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The closo -Ge 52- Anion: Synthesis, Crystal Structure, and Raman Spectrum of (2,2,2-crypt-K + ) 2 Ge 52- ·THF

✍ Scribed by Campbell, Janette; Schrobilgen, Gary J.

Book ID
127286984
Publisher
American Chemical Society
Year
1997
Tongue
English
Weight
139 KB
Volume
36
Category
Article
ISSN
0020-1669

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✍ Mehmet Somer; Wilder Carrillo-Cabrera; Eva-Maria Peters; Karl Peters; Martin Kau 📂 Article 📅 1999 🏛 John Wiley and Sons 🌐 German ⚖ 211 KB 👁 1 views

Dark red crystals of [K-(2,2,2)-crypt)] 2 Sn 5 precipitate after the reaction of (2,2,2)-crypt with a solution of K 1.33 Sn in liquid ammonia at room temperature. The compound is sensitive to oxidation and hydrolysis. The sequence of Raman bands (104, 120, 133 and 180 cm ±1 ) is characteristic for t