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The Cleavage of (Dialkylvinyl)-alkylcyanoacetic Esters by Sodium Alkoxides 1

✍ Scribed by Osman, Elizabeth M.; Cope, Arthur C.


Book ID
126009037
Publisher
American Chemical Society
Year
1944
Tongue
English
Weight
767 KB
Volume
66
Category
Article
ISSN
0002-7863

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## Abstract A method for the determination of total 3‐chloropropane‐1,2‐diol (3‐MCPD) in edible fats and oils was presented. 3‐MCPD was released from 3‐MCPD fatty acid esters by transesterification with NaOCH~3~/methanol. After derivatization with phenylboronic acid, 3‐MCPD was determined by GC‐MS.