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The Chemistry of Dichloro[phthalocyaninato(2-)]titanium(IV)

✍ Scribed by Block, B. P.; Meloni, E. G.

Book ID
126306974
Publisher
American Chemical Society
Year
1965
Tongue
English
Weight
277 KB
Volume
4
Category
Article
ISSN
0020-1669

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Synthesis, X-ray crystal structure and reactivity of dichloro(phthalocyaninato)niobium(IV) (new polymorph) and trichloro(phthalocyaninato)niobium(V)
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Dichloro(phthalocyaninato)niobium(IV), PcNbCl 2, has been isolated as a new polymorph and its X-ray crystal structure solved. Crystals are triclinic: formula C 32 H 16 Cl 2 N 8 Nb , space group P1, cell parameters a = 8.707(2) Å, b = 12.288(3) Å, c = 12.801(3) Å, α = 80.72(2) °, β = 85.43(2) °, γ =