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The calibration of disc-type laboratory gas-absorption columns

✍ Scribed by R.F. Taylor; F. Roberts


Book ID
103002933
Publisher
Elsevier Science
Year
1956
Tongue
English
Weight
735 KB
Volume
5
Category
Article
ISSN
0009-2509

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✦ Synopsis


The disc column [17, 121 has been examined from the calibration standpoint, using two systems : carbon dioxide into water, and dilute ammonia gas into water. The plots of film coefficient versus liquid rate show a distinct change of slope, not previously reported ; this break coincides with the establishment of ripple formation on the rims of the 'discs. The film coefficients were consistently below those of STEPHENS and Moruus, but differences in calibration between different disc columns are not uncommon. Some workers have found it difficult to wet the discs successfully. However, in this work wettiug was successfully aebieved by systematically roughening pyrophyllite discs, and keeping them wet between runs. RBsum6-Les auteurs ont etudie l'etalonnage d'une colonne a disques [17, 121 au moyen des deux systtmes : CO, dans l'eau et ammoniac dilue dans l'eau. Les courbes du coefficient laminaire d'ecbange en fonction de la vitesse du liquide montrent une variation nette de la pente qui n'a pas et6 signal&e ; cette cassure coincide avec la formation de rides sur le bord des diquses. Les coefficients sont sensiblement inferieurs ir ceux de STEPHENS et MORRIS, mais il y a suuvent des differences dans le calibrage des disques de colonnes que certains auteurs ont Bprouvt! des difficultes a mouiller correctement. Un mouillage parfait a et6 obtenu dans le cas des disques de pyrophyllite, grace ir un depolissage systematique et la conservation B petat mouille entre les experiences.


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