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The biosynthetic prepartion of 1-14C -trans-11-octadecenoic acid

✍ Scribed by W. W. Christie; M. L. Hunter; C. G. Harfoot

Book ID
102369355
Publisher
John Wiley and Sons
Year
1973
Tongue
French
Weight
180 KB
Volume
9
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

l‐^14^C‐Trans‐11‐octadecenoic acid was obtained in 60% overall yield by incubating 1‐^14^C ‐linoleic acid with sheep rumen microorganisms. The product, purified in the form of the methyl ester by silver nitrate chromatography, contained small amounts of related positional isomere as the only impurities.

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Preparation of [1-14C]- and [9,10-3H]-Tr
Preparation of [1-14C]- and [9,10-3H]-Trans-9-Octadecenoic Acids from the Corresponding cis-Compounds
✍ William W. Christie πŸ“‚ Article πŸ“… 1979 πŸ› John Wiley and Sons 🌐 French βš– 168 KB

l-'4C]-Trans-9-octadecenoic acid was obtained in 60 per cent overall yield and [9, 10-3H]-trans-9-octadecenoic acid in 30 per cent yield by stereomutation of the double bonds in the corresponding cis-compounds with nitrous acid in toluene. purified by silver nitrate chromatography and contained no