Preparation of [1-14C]- and [9,10-3H]-Trans-9-Octadecenoic Acids from the Corresponding cis-Compounds
โ Scribed by William W. Christie
- Publisher
- John Wiley and Sons
- Year
- 1979
- Tongue
- French
- Weight
- 168 KB
- Volume
- 16
- Category
- Article
- ISSN
- 0022-2135
No coin nor oath required. For personal study only.
โฆ Synopsis
l-'4C]-Trans-9-octadecenoic acid was obtained in 60 per cent overall yield and [9, 10-3H]-trans-9-octadecenoic acid in 30 per cent yield by stereomutation of the double bonds in the corresponding cis-compounds with nitrous acid in toluene.
purified by silver nitrate chromatography and contained no detectable positional isomers.
๐ SIMILAR VOLUMES
## Abstract The complete ^1^H NMR chemical shift assignments of 1,2,3,4,5,6,7,8โoctahydroacridine (**1**), 1,2,3,4,5,6,7,8โoctahydroโ9โ(3โpyridyl)acridine (**2**), 1,2,3,4,5,6,7,8โoctahydroโ9โ(4โpyridyl)acridine (**3**) and the corresponding __N__(10)โoxides **1a**, **2a** and **3a**, respectively,