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The Baeyer–Villiger Oxidation with Trifluoroacetic Acid and Household Sodium Percarbonate

✍ Scribed by Kjonaas, Richard A.; Clemons, Anthony E.

Book ID
120474028
Publisher
American Chemical Society
Year
2008
Tongue
English
Weight
187 KB
Volume
85
Category
Article
ISSN
0021-9584

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✍ Albrecht Berkessel; Marc R.M Andreae 📂 Article 📅 2001 🏛 Elsevier Science 🌐 French ⚖ 55 KB

We have found that the Baeyer-Villiger oxidation of cyclohexanone with hydrogen peroxide in 1,1,1,3,3,3-hexafluoro-2propanol as solvent is catalyzed by Brønsted acids: in the presence of 1 mol% of p-TsOH, transformation to o-caprolactone occurs rapidly and under mild conditions. Epoxidation of 1-oct