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The 14N NQR spectrum and the crystal structure of Ba[Fe(CN) 5NO] · 3H2O at room temperature

✍ Scribed by Juan Murgich; Ismardo Bonalde


Publisher
Elsevier Science
Year
1990
Tongue
English
Weight
290 KB
Volume
75
Category
Article
ISSN
0038-1098

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The novel thioantimonate(III) [Fe(C 4 H 13 N 3 ) 2 ]Sb 6 S 10 • 0.5 H 2 O was synthesised under mild hydrothermal conditions by allowing elemental Fe, Sb, and S to react in a 50% diethylenetriamine (dien) solution. The compound crystallises in the monoclinic space group C2/c with a = 33.789(3), b =