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Tetrasilacyclobutadiene (tBu2MeSi)4Si4: A New Ligand for Transition-Metal Complexes.

✍ Scribed by Kazunori Takanashi; Vladimir Ya. Lee; Tadahiro Matsuno; Masaaki Ichinohe; Akira Sekiguchi

Publisher
John Wiley and Sons
Year
2005
Weight
8 KB
Volume
36
Category
Article
ISSN
0931-7597

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Section 3: Compound 4 [4] (80 mg, 0.075 mmol) and KC 8 (22 mg, 0.163 mmol) were placed in a reaction tube with a magnetic stirrer. Oxygen-free, dry THF (2 mL) was introduced into the reaction tube by vacuum transfer, and the reaction mixture was stirred at room temperature to produce a yellow soluti

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A (Tetrasilacyclobutadiene)tricarbonyliron Complex [{Ξ·4-(tBu2MeSi)4Si4}Fe(CO)3]: The Silicon Cousin of Pettit's (Cyclobutadiene)tricarbonyliron Complex [(Ξ·4-H4C4)Fe(CO)3]
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## Experimental Section 3: Compound 4 [4] (80 mg, 0.075 mmol) and KC 8 (22 mg, 0.163 mmol) were placed in a reaction tube with a magnetic stirrer. Oxygen-free, dry THF (2 mL) was introduced into the reaction tube by vacuum transfer, and the reaction mixture was stirred at room temperature to produ