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Tetra-n-butyl­ammonium hexa­fluoro­phosphate at 110 K

✍ Scribed by Stein, Zafra ;Goldberg, Israel

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
184 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

Single-crystal X-ray study T = 110 K Mean '(C±C) = 0.003 A Ê R factor = 0.048 wR factor = 0.130 Data-to-parameter ratio = 21.9

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Tetra-n-butyl­ammonium hexa­fluoro­phosp
Tetra-n-butyl­ammonium hexa­fluoro­phosphate
✍ Schödel, Frauke ;Lerner, Hans-Wolfram ;Bolte, Michael 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 252 KB

The structure of the title compound, C 16 H 36 N + ÁPF 6 À , has been reported previously by Angaridis, Cotton & Petrukhina [Inorg. Chim. Acta (2001), 324, 318±323]. However, these authors found the PF 6 À ion to be heavily disordered and they did not publish any coordinates. We present here a redet