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Tethered Dithiacyclopropenones. Syntheses and Structural Properties of Tetrathiacyclopropenonophanes

✍ Scribed by Werz, Daniel B.; Rominger, Frank; Hyla-Kryspin, Isabella; Gleiter, Rolf

Book ID
125991319
Publisher
American Chemical Society
Year
2001
Tongue
English
Weight
99 KB
Volume
66
Category
Article
ISSN
0022-3263

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The four-component cyclization of dilithium acetylide with dithiocyanatoalkanes yielded the hitherto unknown tetrathiacyclodiynes 34, 38, 41, and 43 in moderate yields. The use of the trimethylsilyl protecting group allowed a more efficient and flexible stepwise approach with good yields. The result