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Syntheses and Structural Properties of Distellenes

✍ Scribed by Gleiter, Rolf; Fritzsche, Gerd; Borzyk, Oliver; Oeser, Thomas; Rominger, Frank; Irngartinger, Hermann

Book ID
126034942
Publisher
American Chemical Society
Year
1998
Tongue
English
Weight
150 KB
Volume
63
Category
Article
ISSN
0022-3263

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The four-component cyclization of dilithium acetylide with dithiocyanatoalkanes yielded the hitherto unknown tetrathiacyclodiynes 34, 38, 41, and 43 in moderate yields. The use of the trimethylsilyl protecting group allowed a more efficient and flexible stepwise approach with good yields. The result