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Terminal and Bridging Parent Amido 1,5-Cyclooctadiene Complexes of Rhodium and Iridium

✍ Scribed by Mena, Inmaculada; Jaseer, E. A.; Casado, Miguel A.; García-Orduña, Pilar; Lahoz, Fernando J.; Oro, Luis A.

Book ID
120411320
Publisher
John Wiley and Sons
Year
2013
Tongue
English
Weight
433 KB
Volume
19
Category
Article
ISSN
0947-6539

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Treatment of [[M(mu-Cl)(diolefin)](2)] with the lithium salts of primary and secondary amines (LiNRR') in diethyl ether affords the complexes [[M(mu-NRR')(diolefin)](2)] (M=Rh, Ir; diolefin=1,5-cyclooctadiene (cod), tetrafluorobenzobarrelene (tfb); R'=H, R=tBu, Ph, 4-MeC(6)H(4); R=R'=Ph, 4-MeC(6)H(4