The curing behavior of a self-crosslinkable polyacrylate coating system was studied by torsion braid analysis (TBA), thermogravimetric analysis (TGA), and in situ Fourier transform infrared (FTIR). The results of heating TBA showed that the curing process consisted of two stages: The first stage was
TBA studies of prepreg curing behavior
โ Scribed by N. S. Schneider; J. K. Gillham
- Book ID
- 104510877
- Publisher
- Society for Plastic Engineers
- Year
- 1980
- Tongue
- English
- Weight
- 452 KB
- Volume
- 1
- Category
- Article
- ISSN
- 0272-8397
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โฆ Synopsis
Abstract
The torsional braid analysis (TBA) equipment has been used as an automated torsion pendulum to characterize prepreg materials in the form of single ply strips (2โ1/2 ร 1/8 in.). Compared to the use of coated glass braids, the main difference was a marked weakening of the gelation mechanical damping peak in isothermal runs. However, prepreg materials consisting of epoxy resins on glass, carbon or aramid fibers were successfully run isothermally to provide gelation and vitrification times as a function of temperature, or in constant heating rate scans to reveal the T < T~g~ and the T~g~ relaxations of the uncured resins, and at higher temperatures phenomena associated with gelation, vitrification and devitrification.
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## Abstract The curing process of epoxy prepreg was studied by means of differential scanning calorimetry analysis. The dynamic, isothermal, and combinations of dynamic and isothermal measurements were done over selected temperature ranges and isothermal cure temperatures. The heats of reaction for