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Synthesis, x-ray crystal structure and multistage redox properties of a severely-distorted tetrathiafulvalene donor

✍ Scribed by Martin R. Bryce; Malcolm A. Coffin; Michael B. Hursthouse; A.I. Karaulov; Klaus Müllen; Harald Scheich

Book ID
108381456
Publisher
Elsevier Science
Year
1991
Tongue
French
Weight
254 KB
Volume
32
Category
Article
ISSN
0040-4039

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Tetrathiafulvalene (TTF) fused to acenap
Tetrathiafulvalene (TTF) fused to acenaphthyleno[1,2b][1,4]dithiine: synthesis and X-ray crystal structure of a new π-electron donor system
✍ Martin R. Bryce; Alexander K. Lay; Andrei S. Batsanov; Judith A.K. Howard 📂 Article 📅 1999 🏛 Elsevier Science 🌐 French ⚖ 210 KB

The reaction of transient 1,3-dithiole-2,4,5-trithioue 4 with acenaphthylene afforded the Diels-Alder adduct 5, which was dehydrogenated to yield 6; cross-coupling of 6 with 7 gave the tetrathiafulvalene (TIT) derivative 8, which was converted into the di(methylsulfanyl) analogue 10, the solution el