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Synthesis through oxyplumbation. Reaction of styrene with acetylacetone in the presence of lead tetraacetate

✍ Scribed by Ichikawa, Katsuhiko; Uemura, Sakae


Book ID
126941299
Publisher
American Chemical Society
Year
1967
Tongue
English
Weight
357 KB
Volume
32
Category
Article
ISSN
0022-3263

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Synthesis of 1,4-diketones by the coupli
✍ Robert M. Moriarty; Raju Penmasta; Indra Prakash πŸ“‚ Article πŸ“… 1987 πŸ› Elsevier Science 🌐 French βš– 183 KB

Synthesis of 1,4-diketones in good yields was achieved by the coupling reaction of the trinethylsilyl enol ethers of acetophenone, thiophene or furan with lead tetraacetate in dry dichloromethane and tetrahydrofuran at -78"C.