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Synthesis, Structure, and Reactivity of a Stabilized Phosphiranylium Salt

✍ Scribed by Helen Jansen; Florian B. Läng; J. Chris Slootweg; Andreas W. Ehlers; Martin Lutz; Koop Lammertsma; Hansjörg Grützmacher

Publisher: John Wiley and Sons
Year: 2010
Tongue: English
Weight: 424 KB
Volume: 49
Category: Article
ISSN: 0044-8249
DOI: 10.1002/anie.201000901

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tive towards S8, CH2N2, Fez(C0)9, and CS,; 1Oa-c and 11 are formed. Variable temperature 'H-NMR spectro-10 11 a , X = S ; b, X = CHZ; c , X = F e ( C 0 ) 4 scopic studies on 10a-c indicate that a rapid "olefinlike" rotation of the (Me2N)2P-X moiety occurs[' 'I.